Prep HPLC Column, UDC Cholesterol, 4um, 100A. 30mm ID x 250mm Length, Preparative. Cogent TYPE-C Brand. 1 EA.

Additional Info:

The 69069‑P30‑250 Cogent UDC‑Cholesterol Preparative HPLC Column is engineered for maximum separation performance at the largest purification scale, utilizing 4 µm TYPE‑C™ silica hydride particles modified with a cholesterol‑terminated ligand to deliver unique shape‑based selectivity.

This stationary phase features an 11‑carbon chain directly bonded to silica hydride with a terminal cholesterol group, forming structured interaction regions that act as molecular “slots.” These allow compounds to be separated based on molecular geometry, steric orientation, and shape, in addition to hydrophobic interaction—making it highly effective for closely related compounds, positional isomers, and complex mixtures.

Key advantages:

  • Direct Si–C bonding (no end‑capping required)

  • Reduced silanol activity and secondary interactions

  • Enhanced durability and reproducibility under high‑load conditions

Supports multiple chromatographic modes:

  • Reversed Phase

  • Normal Phase

  • HILIC

Preparative Column Use‑Case Framework

250 mm Length – Maximum Separation & Peak Capacity

  • Highest resolving power in the 30 mm preparative column range

  • Maximizes peak capacity for highly complex mixtures

  • Ideal for final purification and ultra‑high‑purity fraction collection

  • Best suited for closely related isomers and difficult separations

  • Longest run times compared to 50 mm, 100 mm, and 150 mm formats

Flow Rate & System Requirements (30 mm ID)

Large‑scale preparative columns require specialized high‑flow systems

  • Typical flow rate range: ~40 – 120 mL/min

  • Optimal starting range: ~35 – 70 mL/min for maximum resolution

  • Requires:

    • Preparative HPLC system with high‑flow capability

    • High‑capacity pump heads, tubing, and fittings

    • Fraction collection system

    • Proper solvent handling infrastructure

⚠️ Standard analytical HPLC systems are not suitable for this column size.

Flow optimization depends on:

  • Sample load and injection volume

  • Desired resolution vs throughput

  • Solvent viscosity

  • System pressure limits

Why Choose UDC‑Cholesterol™ for Preparative Work

Shape‑Selective Purification

  • Separates analytes based on 3D structure and steric interaction

  • Ideal for isolating closely related isomers

Strong Hydrophobic Interaction

  • Highly hydrophobic stationary phase

  • Effective retention for lipids and difficult compounds

Tunable Selectivity

  • Adjust separation conditions using:

    • Temperature changes

    • Mobile phase composition

  • Enables precise purification control

Cogent TYPE‑C™ Technology Advantages

Silica Hydride Surface

  • Direct Si–C bonding eliminates end‑capping requirement

  • Reduced secondary interactions

  • Improved peak shape and recovery

Faster Equilibration

  • Shorter cycle times

  • Increased purification throughput

Robust Column Lifetime

  • Resistant to hydrolysis

  • Stable under high‑flow, high‑load conditions

  • Long operational durability

Typical Applications

  • Large‑scale purification of steroidal compounds

  • Isolation of structural isomers

  • Lipids and highly hydrophobic analytes

  • Peptides, proteins, and oligonucleotides

  • Complex multi‑component mixtures

  • Final purification where maximum separation is required

  • Applications where C18/C8 phases lack sufficient selectivity

Important Usage Notes

  • Requires a full preparative HPLC system

  • Designed for high‑flow, high‑load purification workflows

  • Ideal for maximum separation and highest purity isolation

  • Optimize temperature and mobile phase to fine‑tune selectivity

Made‑to‑Order & Pricing Information

This is a custom, made‑to‑order item.

  • Orders cannot be canceled once placed

  • Custom items are non‑returnable

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