Prep HPLC Column, UDC Cholesterol, 4um, 100A. 30mm ID x 100mm Length, Preparative. Cogent TYPE-C Brand. 1 EA.

Additional Info:

The 69069‑P30‑100 Cogent UDC‑Cholesterol Preparative HPLC Column is designed for high‑capacity purification with enhanced resolution, using 4 µm TYPE‑C™ silica hydride particles modified with a cholesterol‑terminated ligand to deliver unique shape‑based selectivity.

This stationary phase features an 11‑carbon chain directly bonded to silica hydride with a terminal cholesterol group, forming structured interaction regions that act as molecular “slots.” These interactions allow analytes to be separated based on molecular geometry, steric fit, and shape, in addition to hydrophobic interaction—making it especially effective for closely related compounds and isomers.

Key advantages:

  • Direct Si–C bonding (no end‑capping required)

  • Reduced silanol activity and secondary interactions

  • Enhanced durability and reproducibility under preparative conditions

Supports multiple chromatographic modes:

  • Reversed Phase

  • Normal Phase

  • HILIC

Preparative Column Use‑Case Framework

100 mm Length – Increased Resolution Purification

  • Higher resolving power than 50 mm columns

  • Improved fraction purity and separation of closely related compounds

  • Balanced performance between throughput and resolution

  • Ideal for analytical‑to‑preparative method scale‑up

Flow Rate & System Requirements (30 mm ID)

Large‑scale preparative columns require specialized high‑flow systems

  • Typical flow rate range: ~40 – 120 mL/min

  • Optimal starting range: ~40 – 80 mL/min for enhanced resolution

  • Requires:

    • Preparative HPLC system with high‑flow capability

    • High‑capacity pump heads, tubing, and fittings

    • Fraction collection system

⚠️ Standard analytical HPLC systems are not suitable for this column size.

Flow rates should be optimized based on:

  • Sample load and injection volume

  • Desired resolution vs throughput

  • Mobile phase viscosity

  • System pressure limitations

Why Choose UDC‑Cholesterol™ for Preparative Work

Shape‑Selective Purification

  • Separates analytes based on 3D structure and steric interaction

  • Ideal for isolating closely related isomers

Strong Hydrophobic Interaction

  • Highly hydrophobic phase

  • Effective retention of lipids and difficult compounds

Tunable Selectivity

  • Optimize separations by adjusting:

    • Temperature

    • Mobile phase composition

  • Enables precise purification control

Cogent TYPE‑C™ Technology Advantages

Silica Hydride Surface

  • Direct Si–C bonding (no end‑capping required)

  • Reduced secondary interactions

  • Improved peak shape and recovery

Faster Equilibration

  • Shorter cycle times

  • Increased purification throughput

Robust Column Lifetime

  • Resistant to hydrolysis

  • Stable under high‑load, high‑flow conditions

  • Long operational durability

Typical Applications

  • Preparative purification of steroidal compounds

  • Isolation of structural isomers

  • Lipids and hydrophobic analytes

  • Peptides, proteins, and oligonucleotides

  • Analytical‑to‑prep method scale‑up

  • Applications where C18/C8 phases lack selectivity

Important Usage Notes

  • Requires a preparative HPLC system

  • Designed for high‑flow, high‑load purification workflows

  • Ideal for balanced purification (resolution + throughput)

  • Optimize temperature and mobile phase to control selectivity

Made‑to‑Order & Pricing Information

This is a custom, made‑to‑order item.

  • Orders cannot be canceled once placed

  • Custom items are non‑returnable

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